» Articles » PMID: 39771325

A Study on the Preparation and Performance of Ultrafine Powder Made of Industrial Hemp Degumming Residue

Overview
Publisher MDPI
Date 2025 Jan 8
PMID 39771325
Authors
Affiliations
Soon will be listed here.
Abstract

Industrial hemp, one of the most widely available and extensively produced varieties, generates a substantial amount of waste in the form of hemp cellulose. This study uses a recycling method combining crushing and acid treatment to convert leftover hemp fiber into ultrafine powder. A scanning electron microscope (SEM), an atomic force microscope (AFM), Fourier transform infra-red spectroscopy (FTIR), and X-ray diffraction (XRD) were used to examine the morphology of acid-treated hemp fiber heated to 200 °C and crushed into powder. The decrease in intensity, fiber surface crystalline, and grain size was analyzed. It became apparent that fiber strength decreased, and fiber roughness significantly increased after acid treatment. The degree of crystallinity of the broken fibers decreased significantly. The proposed method was a simple and effective method for converting leftover hemp fiber into ultrafine powder. In approximately 3 to 5 min, about 1 kg of dry ultrafine powder with a particle size of 38.68 μm was produced. This production method will significantly enhance future industrial applications of hemp residue.

References
1.
Wimalasiri E, Jahanshiri E, Syaherah T, Kuruppuarachchi N, Chimonyo V, Azam-Ali S . Datasets for the development of hemp ( L.) as a crop for the future in tropical environments (Malaysia). Data Brief. 2022; 40:107807. PMC: 8762045. DOI: 10.1016/j.dib.2022.107807. View

2.
Gan L, Guo H, Xiao Z, Jia Z, Yang H, Sheng D . Dyeing and Characterization of Cellulose Powder Developed from Waste Cotton. Polymers (Basel). 2019; 11(12). PMC: 6960988. DOI: 10.3390/polym11121982. View

3.
Liu Y, Wei Y, He Y, Qian Y, Wang C, Chen G . Large-Scale Preparation of Carboxylated Cellulose Nanocrystals and Their Application for Stabilizing Pickering Emulsions. ACS Omega. 2023; 8(17):15114-15123. PMC: 10157680. DOI: 10.1021/acsomega.2c08239. View

4.
Jiang H, Nie J, Zeng L, Zhu F, Gao Z, Zhang A . Selective Removal of Hemicellulose by Diluted Sulfuric Acid Assisted by Aluminum Sulfate. Molecules. 2024; 29(9). PMC: 11085920. DOI: 10.3390/molecules29092027. View

5.
De Silva R, Byrne N . Utilization of cotton waste for regenerated cellulose fibres: Influence of degree of polymerization on mechanical properties. Carbohydr Polym. 2017; 174:89-94. DOI: 10.1016/j.carbpol.2017.06.042. View