Robert E Synovec
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Explore the profile of Robert E Synovec including associated specialties, affiliations and a list of published articles.
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153
Citations
874
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Recent Articles
1.
Ma W, Halvorsen R, Cain C, Synovec R
J Chromatogr A
. 2024 Aug;
1732:465220.
PMID: 39106664
Partial least squares (PLS) regression is a valuable chemometric tool for property prediction when coupled with gas chromatography (GC). Since the separation run time and stationary phase selection are crucial...
2.
Cain C, Synovec R
Talanta
. 2024 Jun;
278:126453.
PMID: 38908137
Chemometric decomposition methods like multivariate curve resolution-alternating least squares (MCR-ALS) are often employed in gas chromatography-mass spectrometry (GC-MS) to improve analyte identification and quantitation. However, these methods can perform poorly...
3.
Mikaliunaite L, Synovec R
J Chromatogr A
. 2024 Jun;
1730:465093.
PMID: 38897109
Herein, two "orthogonal" characteristics of moisture damaged cacao beans (temporally dependent molding kinetics versus the time-independent geographical region of origin) are simultaneously analyzed in a comprehensive two-dimensional (2D) gas chromatography...
4.
Schoneich S, Cain C, Sudol P, Synovec R
J Chromatogr A
. 2023 Sep;
1708:464341.
PMID: 37660566
Comprehensive three-dimensional (3D) gas chromatography with time-of-flight mass spectrometry (GC-TOFMS) is a promising instrumental platform for the separation of volatiles and semi-volatiles due to its increased peak capacity and selectivity...
5.
Gaida M, Cain C, Synovec R, Focant J, Stefanuto P
Anal Chem
. 2023 Aug;
95(36):13519-13527.
PMID: 37647642
In this study, we introduce a new nontargeted tile-based supervised analysis method that combines the four-grid tiling scheme previously established for the Fisher ratio (F-ratio) analysis (FRA) with the estimation...
6.
Ochoa G, Synovec R
Talanta
. 2023 Apr;
259:124525.
PMID: 37031541
Solid phase extraction (SPE) sample preparation for the analysis of complex organic mixtures is often applied assuming all analytes of interest will preconcentrate on the stationary phase. This assumption ignores...
7.
Cain C, Ochoa G, Synovec R
J Chromatogr A
. 2023 Mar;
1694:463920.
PMID: 36933463
Chemometric methods like partial least squares (PLS) regression are valuable for correlating sample-based differences hidden in comprehensive two-dimensional gas chromatography (GC × GC) data to independently measured physicochemical properties. Herein,...
8.
Trinklein T, Cain C, Ochoa G, Schoneich S, Mikaliunaite L, Synovec R
Anal Chem
. 2023 Jan;
95(1):264-286.
PMID: 36625122
No abstract available.
9.
Schoneich S, Cain C, Freye C, Synovec R
Anal Chem
. 2022 Dec;
95(2):1513-1521.
PMID: 36563309
Nontargeted analyses of low-concentration analytes in the information-rich data collected by liquid chromatography with high-resolution mass spectrometry detection can be challenging to accomplish in an efficient and comprehensive manner. The...
10.
Halvorsen R, Trinklein T, Warren C, Rogan R, Synovec R
Talanta
. 2022 Dec;
254:124173.
PMID: 36512972
We examine and then optimize alignment of chromatograms collected on nominally identical columns using retention time locking (RTL), an instrumental alignment tool, and software-based alignment using correlation optimized warping (COW)....