Solid-State Synthesis of Water-Soluble Chitosan-g-Hydroxyethyl Cellulose Copolymers

Overview

Journal Polymers (Basel)

Publisher MDPI

Date 2020 Mar 12

PMID 32156039

Citations 4

Authors

Tatiana S Demina

Aisylu V Birdibekova

Eugenia A Svidchenko

Pavel L Ivanov

Anastasia S Kuryanova

Tikhon S Kurkin

Zulfar I Khaibullin

Galina P Goncharuk

Tatiana M Zharikova

Sankarprasad Bhuniya

Christian Grandfils

Peter S Timashev

Tatiana A Akopova

Affiliations

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Abstract

Graft copolymers of chitosan with cellulose ether have been obtained by the solid-state reactive mixing of chitin, sodium hydroxide and hydroxyethyl cellulose under shear deformation in a pilot twin-screw extruder. The structure and composition of the products were determined by elemental analysis and IR spectroscopy. The physicochemical properties of aqueous solutions of copolymers were studied as a function of the composition, and were correlated to the mechanical characteristics of the resulting films to assess the performance of new copolymers as coating materials, non-woven fibrous materials or emulsifiers for interface stabilization during the microparticle fabrication process.

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