P03, the Microfocus and Nanofocus X-ray Scattering (MiNaXS) Beamline of the PETRA III Storage Ring: the Microfocus Endstation

Overview

Journal J Synchrotron Radiat

Date 2012 Jun 21

PMID 22713902

Citations 40

Authors

Adeline Buffet

Andre Rothkirch

Ralph Dohrmann

Volker Korstgens

Mottakin M Abul Kashem

Jan Perlich

Gerd Herzog

Matthias Schwartzkopf

Rainer Gehrke

Peter Muller-Buschbaum

Stephan V Roth

Affiliations

Soon will be listed here.

Abstract

The P03 beamline, also called the microfocus and nanofocus X-ray scattering (MiNaXS) beamline, exploits the excellent photon beam properties of the low-emittance source PETRA III to provide a microfocused/nanofocused beam with ultra-high intensity for time-resolved X-ray scattering experiments. The beamline has been designed to perform X-ray scattering in both transmission and reflection geometries. The microfocus endstation started user operation in May 2011. An overview of the beamline status and of some representative results highlighting the performance of the microfocus endstation at MiNaXS are given.

Citing Articles

Responsive Magnetic Polymer Nanocomposites through Thermal-Induced Structural Reorganization.

Chen Q, Furrer R, Jamilpanah L, Chumakov A, Bulut Y, Harder C ACS Nano. 2025; 19(6):6165-6179.

PMID: 39912791 PMC: 11841046. DOI: 10.1021/acsnano.4c14311.

Tailored Supramolecular Additives to Control the Crystallization Process and Morphology of MAPbI.

Kuhn M, Wenzel F, Greve C, Kreger K, Schwartzkopf M, Schmidt H Small. 2025; 21(9):e2410230.

PMID: 39910842 PMC: 11878263. DOI: 10.1002/smll.202410230.

Suppressed Degradation Process of PBDB-TF-T1:BTP-4F-12-Based Organic Solar Cells with Solid Additive Atums Green.

Li Z, Vagin S, Zhang J, Guo R, Sun K, Jiang X ACS Appl Mater Interfaces. 2025; 17(6):9475-9484.

PMID: 39883833 PMC: 11826503. DOI: 10.1021/acsami.4c21699.

UV Irradiation as a Versatile Low-Temperature Strategy for Fabricating Templated Mesoporous Titania Films.

Pan G, Yin S, Huber L, Li Z, Tian T, Spanier L Small. 2024; 21(5):e2409856.

PMID: 39690833 PMC: 11798364. DOI: 10.1002/smll.202409856.

Printed Thin Magnetic Films via Ternary Hybrid Diblock Copolymer Films Containing Magnetic Iron Oxide and Nickel Nanoparticles.

Everett C, Jiang X, Reus M, Zhong H, Bitsch M, Plank M ACS Appl Mater Interfaces. 2024; 16(51):71060-71069.

PMID: 39661934 PMC: 11672476. DOI: 10.1021/acsami.4c18920.

References

Kaune G, Ruderer M, Metwalli E, Wang W, Couet S, Schlage K . In situ GISAXS study of gold film growth on conducting polymer films. ACS Appl Mater Interfaces. 2010; 1(2):353-60. DOI: 10.1021/am8000727. View

Hol V , Baumbach . Nonspecular x-ray reflection from rough multilayers. Phys Rev B Condens Matter. 1994; 49(15):10668-10676. DOI: 10.1103/physrevb.49.10668. View

Muller-Buschbaum P . Grazing incidence small-angle X-ray scattering: an advanced scattering technique for the investigation of nanostructured polymer films. Anal Bioanal Chem. 2003; 376(1):3-10. DOI: 10.1007/s00216-003-1869-2. View

ONeill , Affrossman , STAMM . Phase Separation and Dewetting of Weakly Incompatible Polymer Blend Films. Macromolecules. 1998; 31(15):5003-9. DOI: 10.1021/ma971802q. View

Renaud G, Lazzari R, Revenant C, Barbier A, Noblet M, Ulrich O . Real-time monitoring of growing nanoparticles. Science. 2003; 300(5624):1416-9. DOI: 10.1126/science.1082146. View

Roth S, Rothkirch A, Autenrieth T, Gehrke R, Wroblewski T, Burghammer M . Spatially resolved investigation of solution cast nanoparticle films by X-ray scattering and multidimensional data set classification. Langmuir. 2010; 26(3):1496-500. DOI: 10.1021/la9037414. View

Barrett R, Faucon M, Lopez J, Cristobal G, Destremaut F, Dodge A . X-ray microfocussing combined with microfluidics for on-chip X-ray scattering measurements. Lab Chip. 2006; 6(4):494-9. DOI: 10.1039/b517055a. View

Martel A, Burghammer M, Davies R, DiCola E, Panine P, Salmon J . A microfluidic cell for studying the formation of regenerated silk by synchrotron radiation small- and wide-angle X-ray scattering. Biomicrofluidics. 2009; 2(2):24104. PMC: 2719262. DOI: 10.1063/1.2943732. View

Moulin J, Roth S, Muller-Buschbaum P . Flow at interfaces: a new device for x-ray surface scattering investigations. Rev Sci Instrum. 2008; 79(1):015109. DOI: 10.1063/1.2816220. View

10.

Rondeau E, Cooper-White J . Biopolymer microparticle and nanoparticle formation within a microfluidic device. Langmuir. 2008; 24(13):6937-45. DOI: 10.1021/la703339u. View

11.

Metwalli E, Moulin J, Perlich J, Wang W, Diethert A, Roth S . Polymer-template-assisted growth of gold nanowires using a novel flow-stream technique. Langmuir. 2009; 25(19):11815-21. DOI: 10.1021/la901432j. View

12.

Buffet A, Abul Kashem M, Schlage K, Couet S, Rohlsberger R, Rothkirch A . Time-resolved ultrathin cobalt film growth on a colloidal polymer template. Langmuir. 2010; 27(1):343-6. DOI: 10.1021/la102900v. View

13.

Li R, Cornaby S, Kamperman M, Smilgies D . Nanocomposite characterization on multiple length scales using µSAXS. J Synchrotron Radiat. 2011; 18(Pt 5):697-701. PMC: 3161816. DOI: 10.1107/S0909049511024873. View

14.

Roth S, Herzog G, Korstgens V, Buffet A, Schwartzkopf M, Perlich J . In situ observation of cluster formation during nanoparticle solution casting on a colloidal film. J Phys Condens Matter. 2011; 23(25):254208. DOI: 10.1088/0953-8984/23/25/254208. View

15.

Otten A, Koster S, Struth B, Snigirev A, Pfohl T . Microfluidics of soft matter investigated by small-angle X-ray scattering. J Synchrotron Radiat. 2005; 12(Pt 6):745-50. DOI: 10.1107/S0909049505013580. View

16.

Kim S, Jinschek J, Chen H, Sholl D, Marand E . Scalable fabrication of carbon nanotube/polymer nanocomposite membranes for high flux gas transport. Nano Lett. 2007; 7(9):2806-11. DOI: 10.1021/nl071414u. View

17.

Korstgens V, Wiedersich J, Meier R, Perlich J, Roth S, Gehrke R . Combining imaging ellipsometry and grazing incidence small angle X-ray scattering for in situ characterization of polymer nanostructures. Anal Bioanal Chem. 2009; 396(1):139-49. DOI: 10.1007/s00216-009-3008-1. View