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7-Chloro-4-[(E)-2-(2-methoxy-benzyl-idene)hydrazin-1-yl]quinoline Monohydrate

Overview
Journal Acta Crystallogr Sect E Struct Rep Online
Date 2011 May 18
PMID 21580438
Citations 8
Authors
Marcus V N de Souza
R Alan Howie
Edward R T Tiekink
James L Wardell
Solange M S V Wardell
Carlos R Kaiser
Affiliations
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Abstract

In the title hydrate, C(17)H(14)ClN(3)O·H(2)O, the dihedral angle between the quinoline fused-ring system and the benzene ring is 13.4 (2)° and the conformation about the C=N bond is E. In the crystal, N(h)-H⋯O(w) and O(w)-H⋯N(q) (h = hydro-zone, w = water and q = quinoline) hydrogen bonds generate a two-dimenstional network in the ac plane. A weak C-H⋯O inter-action helps to consolidate the packing.

Citing Articles

4-[(E)-2-(2-Chloro-benzyl-idene)hydrazin-1-yl]quinolin-1-ium chloride dihydrate.

Tiekink E, Wardell S, Wardell J, de Lima Ferreira M, de Souza M, Kaiser C Acta Crystallogr Sect E Struct Rep Online. 2012; 68(Pt 6):o1850-1.

PMID: 22719616 PMC: 3379418. DOI: 10.1107/S1600536812022660.

7-Chloro-4-[(E)-2-(2,5-dimeth-oxy-benzyl-idene)hydrazin-1-yl]quinoline.

de Souza M, de Lima Ferreira M, Wardell S, Tiekink E, Wardell J Acta Crystallogr Sect E Struct Rep Online. 2012; 68(Pt 4):o1244-5.

PMID: 22606177 PMC: 3344174. DOI: 10.1107/S1600536812012871.

4-[(E)-2-(2,4-Dichloro-benzyl-idene)hydrazin-1-yl]quinolin-1-ium chloride monohydrate.

Wardell S, Tiekink E, Wardell J, de Lima Ferreira M, de Souza M Acta Crystallogr Sect E Struct Rep Online. 2012; 68(Pt 4):o1232-3.

PMID: 22606166 PMC: 3344163. DOI: 10.1107/S1600536812012962.

7-Chloro-4-[(E)-2-(3,4,5-trimeth-oxy-benzyl-idene)hydrazin-1-yl]quinoline.

de Lima Ferreira M, de Souza M, Wardell S, Tiekink E, Wardell J Acta Crystallogr Sect E Struct Rep Online. 2012; 68(Pt 4):o1214-5.

PMID: 22606152 PMC: 3344149. DOI: 10.1107/S1600536812012755.

2-[(E)-Phen-yl(2-phenyl-hydrazin-1-yl-idene)meth-yl]phenol.

Howie R, Wardell J, Wardell S, Tiekink E Acta Crystallogr Sect E Struct Rep Online. 2012; 68(Pt 3):o796-7.

PMID: 22412667 PMC: 3297864. DOI: 10.1107/S1600536812005387.

References
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de Souza M, Tiekink E, Wardell J, Wardell S . 4-[(2-Chloro-ethyl)amino]quinolinium chloride monohydrate. Acta Crystallogr Sect E Struct Rep Online. 2011; 65(Pt 12):o3120-1. PMC: 2971810. DOI: 10.1107/S160053680904834X. View