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Microwave-Enhanced Fluorous Synthesis

Overview
Journal Chim Oggi
Specialty Biochemistry
Date 2007 Dec 15
PMID 18079975
Citations 1
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Abstract

A new technology for high-speed solution-phase parallel synthesis has been developed by the combination of microwave heating and fluorous tagging strategies. This article highlights several applications of this technology in the synthesis of library scaffolds involving Pd-catalyzed cross-coupling and multicomponent reactions.

Citing Articles

Fluorous-enhanced multicomponent reactions for making drug-like library scaffolds.

Zhang W Comb Chem High Throughput Screen. 2007; 10(3):219-29.

PMID: 17346120 PMC: 1857346. DOI: 10.2174/138620707780126697.

References
1.
Zhang W, Lu Y, Chen C . Combination of microwave reactions with fluorous separations in the palladium-catalyzed synthesis of aryl sulfides. Mol Divers. 2004; 7(2-4):199-202. PMC: 1894905. DOI: 10.1023/b:modi.0000006825.12186.5f. View

2.
Kappe C . Controlled microwave heating in modern organic synthesis. Angew Chem Int Ed Engl. 2004; 43(46):6250-84. DOI: 10.1002/anie.200400655. View

3.
Zhang W . Fluorous synthesis of heterocyclic systems. Chem Rev. 2004; 104(5):2531-56. PMC: 1618880. DOI: 10.1021/cr030600r. View

4.
Lu Y, Zhang W . Microwave-assisted synthesis of a 3-aminoimidazo[1,2-a]-pyridine/pyrazine library by fluorous multicomponent reactions and subsequent cross-coupling reactions. QSAR Comb Sci. 2008; 23(10):827-835. PMC: 2423329. View

5.
Nagashima T, Zhang W . Solution-phase parallel synthesis of an N-alkylated dihydropteridinone library from fluorous amino acids. J Comb Chem. 2004; 6(6):942-9. DOI: 10.1021/cc049885r. View