207Pb Chemical Shift Thermometer at High Temperature for Magic Angle Spinning Experiments
Overview
Authors
Affiliations
The temperature dependence of 207Pb chemical shift in magic angle spinning (MAS) NMR spectrum of Pb(NO3)2 provides a sensitive method to calibrate sample temperatures in MAS NMR. The temperature dependence is uniform in the temperature range between 30 degrees C and 400 degrees C. The NMR sensitivity and the line width are also favorable.
Displacive Jahn-Teller Transition in NaNiO.
Nagle-Cocco L, Genreith-Schriever A, Steele J, Tacconis C, Bocarsly J, Mathon O J Am Chem Soc. 2024; 146(43):29560-29574.
PMID: 39401126 PMC: 11528442. DOI: 10.1021/jacs.4c09922.
Solid-State NMR and NQR Spectroscopy of Lead-Halide Perovskite Materials.
Piveteau L, Morad V, Kovalenko M J Am Chem Soc. 2020; 142(46):19413-19437.
PMID: 32986955 PMC: 7677932. DOI: 10.1021/jacs.0c07338.
Rimsza J, Sorte E, Alam T ACS Omega. 2019; 4(1):1033-1044.
PMID: 31459379 PMC: 6648527. DOI: 10.1021/acsomega.8b02705.
NMR Studies of Thermo-responsive Behavior of an Amphiphilic Poly(asparagine) Derivative in Water.
Watanabe E, Boutis G, Sato H, Sekine S, Asakura T Polymer (Guildf). 2015; 55(1):278-286.
PMID: 25614708 PMC: 4299659. DOI: 10.1016/j.polymer.2013.11.015.
A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds.
Guan X, Stark R Solid State Nucl Magn Reson. 2010; 38(2-3):74-6.
PMID: 21036557 PMC: 3008415. DOI: 10.1016/j.ssnmr.2010.10.001.